Feedback system of a liquid nitrogen cooled double-crystal monochromator: design and performances

Olivier Proux 1 Vivian Nassif 2 Alain Prat 3 Olivier Ulrich 2 Eric Lahera 1 Xavier Biquard 2 Jean-Jacques Menthonnex 4 Jean-Louis Hazemann 5
1 équipe FAME
OSUG - Observatoire des Sciences de l'Univers de Grenoble
2 SP2M - UMR 9002 - Service de Physique des Matériaux et Microstructures
3 LC - Laboratoire de cristallographie
4 OSUG - Observatoire des Sciences de l'Univers de Grenoble
5 SPMCE
LC - Laboratoire de cristallographie
Abstract : Abstract We report on a new setup of indirect cryogenic cooling system for double-crystal monochromator running on BM30b / FAME beamline at the ESRF (Grenoble, France). This device has been conceived to limit the vibrations on the first diffracting crystal and to maintain it at a constant temperature. These points are crucial to maximize the beamline stability. Moreover, the relative angular position of the second crystal is dynamically adjusted by a piezoelectric transducer coupled with a feedback system in order to always be at the maximum of the rocking curve during a XAS scan. The temperature is stabilized with a 1/100° accuracy with two principal consequences. The energy resolution is close to the theoretical value (E/E=5.6 10-6 for Si(220)) and the precision of the energy positioning is extremely good even if the power load changes. A feedback mechanism allows a permanent and automatic optimisation of the angle between the two crystals of the monochromator. The intensity of the monochromatic beam remains optimized 1) when the intensity of the electron beam decreases in the storage ring and 2) during an energy scan.
Keywords : double-crystal monochromator cryogenic cooling parallelism adjustment X-ray absorption spectroscopy
Document type :
Journal articles
Journal of Synchrotron Radiation, International Union of Crystallography, 2005, 13 (1), pp.59-68. <10.1107/S0909049505037441>
https://hal-insu.archives-ouvertes.fr/insu-00713235
Contributor : Olivier Proux <>
Submitted on : Friday, June 29, 2012 - 4:08:45 PM
Last modification on : Monday, October 13, 2014 - 3:43:25 PM

File

2006_JSR_Proux.pdf
fileSource_public_greenPublisher

Identifiers

Collections

INSU | CNRS | UGA | INAC-SP2M | DSM-INAC | CEA

Citation

Olivier Proux, Vivian Nassif, Alain Prat, Olivier Ulrich, Eric Lahera, et al.. Feedback system of a liquid nitrogen cooled double-crystal monochromator: design and performances. Journal of Synchrotron Radiation, International Union of Crystallography, 2005, 13 (1), pp.59-68. <10.1107/S0909049505037441>. <insu-00713235>

Export

BibTeX | XML | endNote

Share

Metrics

Consultation de
la notice

127

Téléchargement du document

25

Contact

support.ccsd.cnrs.fr
hal.support@ccsd.cnrs.fr